Cryostat Liquid Nitrogen boil-off rate measurements.

Last update: 15 July 2015

A passive "rotameter" type flow-meter (ball in tapered tube) was found to be sensitive enough to measure the liquid nitrogen (LN2) boil-off rate of a cryostat, leaving enough headroom for fault conditions. Since the boil-off flow-rate of a cryostat is a direct indication of the state of its vacuum or the presence of excessive heat generation inside the cryostat, a measure of this can be used as a diagnostic tool for faultfinding. If the size of the LN2 tank is known, the projected hold time can also be calculated from the knowledge that 1 litre of LN2 produces 648 litres of nitrogen gas.

The flow-meter together with all the necessary fittings and pipes to connect to all the different cryostats in Sutherland are being stored in a box in the CCD cupboard on the 40" observing floor - see pictures below.

Since the array of cryostats used at SAAO all differ somewhat in design, heat load, etc., the boil-off rates under non-fault conditions had to be known first to get an idea of normal conditions. Some of these were measured before using an old gas consumption meter and actual values using the rotameter were taken lately. Typical values are given below. All measurements were with systems powered up (CCD's at controlled temperature where applicable), enough time allowed for the system to stabilise (eg. after a fill) and with the system stationary.


CCD System
Typical
flow-rate
(l/min)
LN2
tank-size
(litre)
Projected
hold time
(Hours)
Notes
see below
Lab measured
hold time
(Hours) *
CCD @ temp.
(Hours) **
CCD Control Temperature (Kelvin) CCD base-
temperature
(Kelvin) ***
IRP II 0.2 - 0.3     Note 1  
IRP III 0.4     Note 1  
TEK6 (10242 - GIRAFFE) 1 - 1.2 1.5 13 - 16 Note 2 >13 (~12 on side) 1.5 180 155
TEK8 (5122) 0.5 - 1.5 1.5 11 - 32 Note 3     180  
SIT1/2 (1752 x 532 - Old SpCCD) 0.55 - 0.8 1.28 17 - 25   23 (18 @ 45°) 2.5 180 165
STE3 (5122, Green) 0.3 - 0.6 1.84 28 - 56 Note 4 28 3 180 148
STE4 (10242, Blue) 0.6 - 0.7 1.84 28 - 33 Note 4 28 >3 180 152
SpUpNIC (2048 x 512 - New Spectrograph CCD) 0.3 - 0.6 1.42 51 - 25.5 Note 4 34 (lab),
29.75 (Suth)
3.5 168 150

* The typical hold time of a system is the time as measured in the lab in its normally used orientation (eg. inverted or upright) with the chip controlled at its working temperature, Zeolite/charcoal intalled, etc.

** The time taken for the CCD (the Cu-block actually) to reach its operation temperature (mostly 180K) after being cooled with LN2, starting from room temperature.

*** The natural temperature the CCD reaches when the temperature control servo is switched off (ie. cu-block not heated).

Notes:

  1. The IRP cryostats take about 4 hours to give a flow reading when the LN2 was being pumped on.
  2. Very little data is available on TEK6. All measurements were with cryostat in upright position (ie. inverted fill tube installed). A flow-rate of 4.2 l/m was measured once before under leak conditions, causing the outer casing to dew up.
  3. The flow-rate on TEK8 shows large variation (under seemingly similar conditions) and was thought to be affected by the ambient temperature.
  4. The projected hold times for all systems were calculated at the min/max flow-rates which are longer than the actual time between fills when the instrument is being used on a moving telescope.

Factors influencing the flow rate.

The flow rate values listed above give the best and worst rates measured so far and should be treated as a guideline to the normal values you could expect. If you find measurements outside this range, please note down the circumstances so that our database can be improved. We are particularly interested in flow-rates under fault conditions - only one instance for TEK6 has been measured yet.

When interpreting a high flow reading, trying to decide the cause, keep the following in mind:


Pictures
Flow Measurement Kit Storage View of the "Flow Measurement Kit", kept in the CCD Cabinet (seen in the background) on the 40" observing floor. Note that the flow meter used for DandiCam is also kept in this cupboard and can be recognised by the marking: "litres/day" - the correct flowmeter to use is the 4 l/min Air as in this picture.
Flow Measurement being taken on SIT1 This picture shows a flow measurement being taken on the (old) Spectrograph Cryostat (SIT1/2) giving a typical flowrate of 0.7 l/min. Note that due to the cryostat neck clamp, the standard IR-Labs fitting cannot be screwed to the cryostat and the rubber bung fitting for DandiCam was used instead.


Raw data.

IRP II

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill. Days since last pump-down.
27/5/1999 11H30 0.4 ±19 4
" 12H30 0.4 ±20 4

IRP III

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill. Days since last pump-down.
28/5/1999 10H45 0.2 ±21 5
" 11H30 0.25 ±22 5
" 14H30 0.3 ±24 5

TEK6 (10242)

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill.

Days since last pump-down.
? 11H20 1.1 2 2
" 14H35 1 5.5 2

TEK8 (5122)

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill.

Days since last pump-down.
10/2/1998 09H00 0.9 10 ?
" 15H00 0.75 10 min ?
11/2/1998 09H30 0.9 10 ?
" 14H00 0.95 14 ?
9/3/1999 09H20 0.95 1 1
" 11H20 0.95 3 1
" 14H50 0.96 14.5 1
" 16H00 1 7 1
29/3/1999 14H10 2 10 min 10 min
" 14H45 1.6 45 min 45 min
" 15H25 1.2 1.5 1.5H
" 16H25 1.1 2.5 2.5H
30/3/1999 09H30 0.9 1.3 1
" 12H45 0.8 4.5 1
" 14H15 0.65 6 1
" 16H00 0.5 8 1
31/3/1999 12H25 1.2 4 2
" 14H15 1.5 6 2
" 15H35 1.5 8 2
1/4/1999 11H30 1.3 3.5 3
" 12H10 1.3 4 3
" 12H55 1.4 5 3
" 14H00 1.4 6 3
" 16H20 1.4 8 3

SIT1/2 (Spectrograph)

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill.

Days since last pump-down.
SIT2 14/8/1996 16H17 0.595 ? ?
SIT1 26/5/1999 11H10 0.75 3 9
" 12H15 0.7 4 9
" 13H05 0.7 4.5 9
" 15H05 0.6 6.5 9
" 15H55 0.6 7.5 9
" 16H15 0.6 8 9
" 16H45 0.7 0.5 9
27/5/1999 08H50 0.55 24 10
" 09H15 0.7 25 min 10
" 14H30 0.8 5.5 10
" 16H40 0.8 8 10

STE4 (Blue)

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill.

Days since last pump-down.
28/1/1999 10H25 0.578 ? ?
" 11H30 0.775 ? ?
27/5/1999 09H45 0.7 2 12
" 11H30 0.6 4 12
" 14H00 0.6 6 12
" 14H20 0.7 20 min 12
30/5/1999 11H00 0.6 3.5 15

STE3 (Green)

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill.

Days since last pump-down.
21/9/1999 14H00 0.5 20 1
" 16H00 0.4 22 1
22/9/1999 10H30 0.6 16.5 2
" 16H00 0.6 22 2
23/9/1999 16H00 0.6 24 3
1/11/1999 ? 0.3 ~5 ~5

SpUpNIC (New Spectrograph)

Date.

Time.

Flow-rate. (l/min)

Hours since last LN2 fill.

Days since last pump-down.
20/6/2015 09H00 0.3 16 1
02/7/2015 10H00 0.35 22 1
20/06/2016 0.3 2
04/07/2016 0.6 ~28 17